Analyzer · Sparsifire

Analyze how specific documents activate the features of the SAE. Select a dataset, a run and a document to begin.

Dataset

SAE Model

Document

Active Features

1512

MIN ACTIVATION

0.0

Details List

#1530 Feature 1530

#1457 Feature 1457

#113 Feature 113

#1526 Feature 1526

#1015 Feature 1015

#1781 Feature 1781

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#1746 Feature 1746

#990 Feature 990

#2577 Feature 2577

#886 Feature 886

#2696 Feature 2696

#404 Interactions and Mechanisms

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#2118 Feature 2118

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#185 Feature 185

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#1065 Feature 1065

#179 Feature 179

#2266 Feature 2266

#1549 Feature 1549

#2523 Feature 2523

#436 Feature 436

#1101 Feature 1101

#2824 Feature 2824

#708 Drug Resistance Mechanisms in Cancer

#2450 Feature 2450

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#1112 Feature 1112

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#873 Feature 873

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#3027 Feature 3027

#351 Nanomaterial Synthesis and Properties

#406 Feature 406

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#264 Feature 264

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#2670 Feature 2670

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#2621 Feature 2621

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#2491 Feature 2491

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#416 Feature 416

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Document Content

Stable 5,5'-Substituted 2,2'-Bipyrroles: Building Blocks for Macrocyclic and Materials Chemistry.
The preparation and characterization of a family of stable 2,2'-bipyrroles substituted at positions 5 and 5' with thienyl, phenyl, TMS-ethynyl, and vinyl groups is reported herein. The synthesis of these new bipyrroles comprises three steps: formation of the corresponding 5,5'-unsubstituted bipyrrole, bromination, and Stille or Suzuki coupling. The best results in the coupling are obtained using the Stille reaction under microwave irradiation. The new compounds have been fully characterized by UV-vis absorption, fluorescence, and IR spectroscopies and cyclic voltammetry. X-ray single-crystal analysis of four of the synthesized bipyrroles indicates a trans coplanar geometry of the pyrrole rings. Furthermore, the substituents at positions 5,5' remain coplanar to the central rings. This particular geometry extends the π-conjugation of the systems, which is in agreement with a red-shifting observed for the λmax of the substituted molecules compared to the unsubstituted bipyrrole. All of these new compounds display a moderate fluorescence. In contrast with unsubstituted bipyrroles, these bipyrroles are endowed with a high chemical and thermal stability and solubility in organic solvents.

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